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Taylor K-1645-5
Taylor K-1645-5
Boiler Test Kit
  
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Taylor K-1645-5
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Taylor K-1645-5

Test Kit for Boiler and Cooling Systems, Alkalinity/Chloride/Orthophosphate/Sulfite

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DROP TEST ALKALINITY - PM/PT

COMPONENTS: 1 x 5067G Instruction 1 x 9198G Sample Tube, Graduated, 25 mL, plastic w/cap and green dot 1 x R-0637-C Methyl Orange Indicator, 2 oz, DB 1 x R-0638G-A Phenolphthalein Indicator (green cap), .75 oz, DB 1 x R-0645-C Total Alkalinity Indicator, 2 oz, DB 1 x R-0687G-C Sulfuric Acid .12N (green cap), 2 oz, DB.

Alkalinity-P/M (Drop Test)

1. Rinse and fill 25 mL sample tube (#9198G) to 25 mL mark with water to be tested.
2. Add 3 drops R-0638G Phenolphthalein Indicator. Swirl to mix. Sample will turn pink if P alkalinity is present--proceed to Step 3. If no pink color, go to Step 4.
3. If pink, add R-0687G Sulfuric Acid .12N dropwise, swirling and counting after each drop, until color changes from pink to colorless. Record drops as P reading. Always hold bottle in vertical position.
4. Add 5 drops R-0637 Methyl Orange Indicator. Swirl to mix. Sample should turn yellow.
5. Continue adding R-0687G Sulfuric Acid .12N dropwise, swirling and counting after each drop, until color just changes from yellow to orange (salmon pink). Record total drops (Steps 3 and 5) as M reading. Always hold bottle in vertical position. 6. Multiply P reading by 10. Record as parts per million (ppm) P alkalinity as calcium carbonate. Multiply M reading by 10. Record as ppm M alkalinity as calcium carbonate.

Alkalinity-P/T (Drop Test)

1. Rinse and fill 25 mL sample tube (#9198G) to 25 mL mark with water to be tested.
2. Add 3 drops R-0638G Phenolphthalein Indicator. Swirl to mix. Sample will turn pink if P alkalinity is present--proceed to Step 3. If no pink color, go to Step 4.
3. If pink, add R-0687G Sulfuric Acid .12N dropwise, swirling and counting after each drop, until color just changes from pink to colorless. Record drops as P reading. Always hold bottle in vertical position.
4. Add 5 drops R-0645 Total Alkalinity Indicator. Swirl to mix. Sample should turn green.
5. Continue adding R-0687G Sulfuric Acid .12N dropwise, swirling and counting after each drop, until color changes from green to red. Record total drops (Steps 3 and 5) as T reading. Always hold bottle in vertical position. 6. Multiply P reading by 10. Record as parts per million (ppm) P alkalinity as calcium carbonate. Multiply T reading by 10. Record as ppm T alkalinity as calcium carbonate.


DROP TEST CHLORIDE

COMPONENTS: 1 x 5067O Instruction 1 x 9198O Sample Tube, Graduated, 25 mL, plastic w/cap and orange dot 1 x R-0630-C Chromate Indicator, 2 oz, DB 1 x R-0638O-A Phenolphthalein Indicator (orange cap), .75 oz, DB 1 x R-0687O-C Sulfuric Acid .12N, (orange cap), 2 oz, DB 1 x R-0706-C Silver Nitrate Reagent, 2 oz, DB.

Chloride (Drop Test)

NOTE: When sulfite content of sample water to be tested exceeds 10 ppm, the sulfite should be oxidized to prevent interference in test. A 25 mL water sample is first adjusted to the appropriate pH, then 1 mL (or 24 drops) of R-0649 3% Hydrogen Peroxide Solution (sold separately) is added and thoroughly mixed. Continue with the rest of the procedure.

1. Rinse and fill 25 mL sample tube (#9198O) to 25 mL mark with water to be tested.
2. Add 2 drops R-0638O Phenolphthalein Indicator. Swirl to mix. If sample turns red, add R-0687O Sulfuric Acid .12N dropwise, swirling after each drop, until color changes from red to colorless.
3. Add 5 drops R-0630 Chromate Indicator. Swirl to mix. Sample should turn yellow.
4. Add R-0706 Silver Nitrate Reagent dropwise, swirling and counting after each drop, until color changes from yellow to milky salmon (brick) red. Always hold bottle in vertical position.

NOTE: Do not add enough R-0706 Silver Nitrate Reagent to give a brown color. First change from yellow to a milky salmon (brick) red is the endpoint. 5. Multiply drops of R-0706 Silver Nitrate Reagent by 10. Record as parts per million (ppm) chloride.


DROP TEST ORTHOPHOSPHATE (HIGH)

COMPONENTS: Orthophosphate (high) 1 x 5067OP Instruction 2 x 2269 Caps, Dispenser, 18 mm, plastic 1 x 4027 Funnel, 58 mm, plastic 1 x 6003 Brush, Test Tube 1 x 6009 Filter Paper, #610, 9.0 cm, 100/box 1 x 9021 Test Tube, Mixing, Calibrated 5, 10, 14, 15, 17.5 mL, glass w/stopper 1 x 9025 Comparator, 2 Standard, Orthophosphate (high), 30 & 60 ppm 2 x R-0601-C Molybdate Reagent, 2 oz 1 x R-0602P-I Stannous Chloride Powder, 10 g.

Orthophosphate (high) (Color Comparison)

1. Filter water to be tested to clarify.
2. Rinse and fill mixing test tube (#9021) to 5 mL mark with filtered sample.
3. Cap R-0601 Molybdate Reagent with 18 mm dispenser cap (#2269). Add R-0601 Molybdate Reagent to 15 mL mark. Stopper and mix. Remove stopper.
4. Add 2 level dippers R-0602P Stannous Chloride Powder. Stopper and mix.
5. Wipe dry and place in hole of comparator. WAIT 1 MINUTE. Read before 10 minutes. 6. Match color in mixing test tube with a color standard. Record as parts per million (ppm) orthophosphate.


DROP TEST pH (LONG RANGE)

COMPONENTS: 1 X 5067pH Instruction 1 x 5425 Comparator, Color Card, pH (long range), 3.0-11.0 1 x 9017 Test Cell, Calibrated 5 mL, square, plastic w/cap 1 x R-1003U-C-DB Long Range Indicator, 2 oz, DB.

pH (long range) (Color Comparison)

1. Rinse and fill 5 mL test cell (#9017) to 5 mL mark with water to be tested.
2. Add 5 drops R-1003U Long Range Indicator. Cap and mix.
3. Place test cell on white area of pH Long Range color card (#5425). Match color in test cell with a color standard. Record as pH units.

DROP TEST SULFITE, SODIUM

COMPONENTS: Sulfite, Sodium 1 x 5067W Instruction 1 x 9198W Sample Tube, Graduated, 25 mL, plastic w/cap and white dot 1 x R-0638W-C Phenolphthalein Indicator (white cap), 2 oz, DB 1 x R-0699-C Iodide Iodate Reagent, 2 oz, DB 1 x R-0725-I Acid Starch Indicator Powder, 10 g Sulfite, Sodium (Drop Test)

1. Collect water to be tested in a clean, preferably large-mouthed, bottle to overflowing. Immediately cap and cool to room temperature.
2. Rinse and fill 25 mL sample tube (#9198W) to 25 mL mark with cooled (room temperature) water to be tested.
3. Add 1 drop R-0638W Phenolphthalein Indicator. Swirl to mix. Sample should turn red.
4. Add R-0725 Acid Starch Indicator Powder, a dipper at a time, swirling after each dipper, until color changes from red to colorless. Add 2 more dippers. Swirl until dissolved.
5. Add R-0699 Iodide Iodate Reagent dropwise, swirling and counting after each drop, until color changes from colorless to a faint but permanent blue. Always hold bottle in vertical position.
6. Multiply drops of R-0699 Iodide Iodate Reagent by 10. Record as parts per million (ppm) sodium sulfite.

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